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Journal of Minerals & Materials Characterization & Engineering, Vol. 10, No.6, pp.553-560, 2011
jmmce.org Printed in the USA. All rights reserved
Effect of Deformation on the Mechanical and Electrical
Properties of Aluminum-Magnesium Alloy
S. O. Adeosun*, O. I. Sekunowo, S.A. Balogun, L.O. Osoba
Department of Metallurgical and Materials Engineering, University of Lagos, Lagos, Nigeria
*Corresponding Author: firstname.lastname@example.org
This paper presents the effect of deformation on the tensile strength, toughness, hardness and
electrical resistance of aluminum 6063 alloy. Cast samples were cold rolled in the range of 0-24
percent thickness reduction and subjected to mechanical (static, dynamic) and electrical
resistance tests. Results show significant improvement in hardness and electrical resistance
properties of the alloy. The nature, amount and distribution of the secondary phase, Mg2Si,
particles precipitated within the matrix which was influenced by the extent of cold-work, are
responsible for the observed behaviour. The resistance of the alloy also depends on the degree of
cold work carried out prior to use.
Keywords: Cold work, tensile strength, toughness, hardness, electrical resistance.
Pure aluminum when subjected to deformation shows an increase in ultimate tensile strength
(UTS), electrical resistance and decrease in toughness and conductivity as the amount of
deformation increased . Aluminum 6063 alloy processed by upset forging and cold rolling at
ambient temperature has shown that the UTS and hardness increase as the range of thickness
reduction suffered increases from 0 to 50 percent while the ductility decreases, an indication of a
low strain-hardening exponent . Cold working of metal causes grain distortion and introduces
imperfection in the crystal structure which affects the electrical property of the alloy.
554 S. O. Adeosun, O. I. Sekunowo, S.A. Balogun, L.O. Osoba Vol.10, No.6
When cold working is combined with heat treatment, it serves the purposes of controlling final
physical/mechanical properties by significantly improving structure homogenizing . Physical
properties such as ductility, strength and toughness are much better in a forged matrix than in the
base metal due to random orientation of crystals . This accounts for preference to some level
of deformation on alloys in order to achieve improved mechanical properties.
There are strong interactions between the solute atoms and defects in aluminum alloys that result
in structural instabilities, variation in solute profiles and changes in solute diffusion rates. Mobile
dislocations are pinned by enhanced solute diffusion during tensile straining due to Portevin-Le
Chatelier (P-L) effect . This phenomenon appears in aluminum alloys over a range of
temperatures above and below room temperature. Plastic deformation not only increases the
mobility of solute atoms in aluminum alloys but also cause clustering at dislocations and these
clusters act as nucleation sites for subsequent strengthening precipitates at temperatures well
below the conventional aging temperatures . This paper investigates the effect of varying
levels of cold work on the mechanical and electrical properties of Al 6063 alloy.
2. EXPERIMENTAL PROCEDURE
Rectangular test samples, 350x30x12mm cast from AA6063 aluminum alloy ingot melted in an
oil fired crucible furnace were used for this study. The chemical composition of the samples is
presented in Table 1.
Table 1: Chemical composition of Cast 6063 aluminum alloy sample.
Element Si Fe Cu Mn Mg Zn Cr Ti Ca Sr Al
The cast samples were machined to 200x30x9 mm and 100x25x9 mm for cumulative and non-
cumulative thickness reduction respectively. The samples were then rolled at ambient
temperature, 250C, using a four-high mill aligned with thickness reduction varying from 0 to 24
percent. The deformed samples hardness was determined using Rockwell Hardness tester type
6402 and the result is shown in Figure 1. Samples were also subjected to impact loading in a
charpy-v test using standard notched impact specimens and the result illustrated in Figure 2.
Otto Wolpert Werke tensometer was used for the tensile test at the rate of 50mm/min and the
results presented in Figure 3. Resistomat type 2319 was used to measure the samples electrical
resistance while the result is illustrated in Figure 4.
Cold rolled samples were prepared for photomicrographic examination by sequential grinding
using emery paper grade 80,220,320 and 600 micron in succession. Etching of the samples for 20
Vol.10, No.6 Effect of Deformation on the Mechanical and Electrical Properties 555
seconds was done using a mixture of dilute nitric acid (68%), hydrofluoric acid (30%), and
sodium hydroxide (2%). Photomicrographs of samples (Plates 1-4) were taken at X200
3. RESULTS AND DISCUSSION
The as-cast sample contains clusters of Mg2Si precipitates that are well-distributed in the α-
aluminum matrix as shown on Plate 1.
Plate 1 Microstructure of as-cast sample (A- α-aluminum, B-Mg2Si)
Rolling the sample at ambient temperature to 4 percent thickness reduction causes most of the
precipitated Mg2Si to be absorbed into the matrix (Plate 2a) exhibiting thin and visible grain
boundaries. There is re-precipitation of fine Mg2Si crystals that are not as coherent as those of
the as-cast with reduced volume fraction at 8 percent reduction (Plate 2b).
Plate 2 Microstructure of as-cast sample (A- α-aluminum, B-Mg2Si)
(a) 4% reduction (b) 8% reduction
However, greater coherency of Mg2Si crystals was observed in sample subjected to 12 percent
reduction with high intensity and high volume fraction when compared to the as-cast (Plate 3a).
556 S. O. Adeosun, O. I. Sekunowo, S.A. Balogun, L.O. Osoba Vol.10, No.6
The intensity and coherency of crystals of Mg2Si is reduced relative to as-cast sample at 16
percent reduction (Plate 3b).
Plate 3 Microstructure of as-cast sample (A- α-aluminum, B- Mg2Si).
(a) 12% reduction (b) 16% reduction
At 20 percent reduction in thickness, clustering and volume fraction of Mg2Si increases (Plate
4a). Processing to 24 percent reduction resulted in increase in fineness of Mg2Si crystal in the α-
aluminum matrix as shown on Plate 4b.
Plate 4 Microstructure of as-cast sample (A- α-aluminum, B-Mg2Si)
(a) 20% reduction (b) 24% reduction
It should be noted that clustering and fineness of crystals increases both the hardness and
strength of cold worked test samples. Similarly, incoherency and coarse crystals in the matrix
and other solute phases promote fracture toughness of the material.
The hardness of test samples increases nearly linearly initially within 0-8 percent thickness
reductions whereas there is no significant increase in hardness between 8 and 14 percent
thickness reduction. At 15 percent and beyond, hardness values increase gradually to the
maximum, 52 HRE, at 24 percent reduction (Figure 1). The reason for this is that at 8-14 percent
Vol.10, No.6 Effect of Deformation on the Mechanical and Electrical Properties 557
reduction, there seems to be temporary saturation in the generation of immobile dislocations as a
result of reduction in the amount of Mg2Si precipitates produced.
3.3 Impact Energy
The test samples behavior under impact loading increases from 0-5 percent thickness reduction,
the maximum energy absorbed, ~880J, occurred at 5 percent reduction (Figure 2).
Impact energy also decreases slowly to a minimum of 425J at about 13 percent reduction.
However, beyond this level of reduction, impact energy increases gradually to 730J with a
tendency to decrease at higher reduction. The minimum of 425J occur at 13 percent reduction in
the domain of immobile dislocation generation saturation. The toughness of a material reduces as
the level of cold work increases .
558 S. O. Adeosun, O. I. Sekunowo, S.A. Balogun, L.O. Osoba Vol.10, No.6
This may be explained using the 16 percent cold work microstructure (Plate 3b) in which the
presence of the second phase precipitates, Mg2Si, reduces progressively at grain boundaries
corresponding to test sample’s percent thickness reduction.
3.4 Tensile Strength
The effect of thickness of samples reduction during deformation at ambient temperature on the
UTS is sinusoidal (Figure 3). The peak tensile strength, 142MPa, occurred at 17 percent
reduction while the minimum of 100MPa was obtained at 23 percent reduction. The non linearity
of the curve at 16 percent cold work is as a result of precipitates of second phase intermetallic,
Mg2Si, which were more pronounced than for other levels of cold work (Plate 2a, 2b, 3a, 4a and
4b). According to Li and Ghosh , uniaxial tensile test usually serve as a major screening for
ranking relative strength of alloy deformation behaviour. Hence, there are more clustering of the
second phase crystals within the matrix in tandem with percent thickness reduction sequence.
3.5 Electrical Resistance
The electrical resistance of test samples after deformation shows a near linear relationship with
thickness reduction for reduction in the ranges from 5-24 percent (non-cumulative). However,
the increase in resistance is rather slow as reduction increases (Figure 4).
Vol.10, No.6 Effect of Deformation on the Mechanical and Electrical Properties 559
In the as-cast state the resistance is ~0.07Ω but rises steadily to a maximum value of 0.08 Ω at 24
percent reduction. Graphical representation of the non-cumulative and cumulative test result
shows that the electrical resistance of aluminum alloy 6063 increase with increased cold work.
This is because the resistance of a material does not only depend on the length but also on
imperfections such as the distribution of second phase crystals and the volume fraction of matrix
constituents in the material .
The study conducted revealed that cold working of 6063 aluminum alloy impacts significant
effects on its mechanical and electrical properties. It has been shown that hardness and resistance
increased from 0 to 24 percent thickness reduction. Substantial improvement in toughness,
strength, hardness and low resistance to current flow is feasible at a thickness reduction in the
neighborhood of 5 percent. At this level of reduction, most of the precipitated Mg2Si crystals are
absorbed into the matrix and there is increase in homogeneity of solution as it becomes more
isotropic. Though the degree of deformation has significant effect on the conductivity of the
alloy however, this will be impaired if the material is made to suffer severe deformation.
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